Samarra Journal of Pure and Applied Science

Four complexes of ionic zinc (II) and cadmium (II) were prepared with ibuprofen ligand (HIbu) and mefenamic acid (Hmef) in the basic medium forming complexes with the formula [M(Ibu)2] and [M(mef)2] where (M=Cd or Zn) Ibu and mef ligands coordinated bi-dental chelate formation to form a tetrahedral shape around the central ion, and the biological activity of the prepared complexes against Bacterium was assessed. The prepared complexes were characterized using infrared spectroscopy, proton and carbon nuclear magnetic resonance, and molar conductivity. Staphylococcus aurous, and the results showed that the produced complexes' activity increased with increasing concentration. Also, the cadmium (II) complexes had greater activity than the zinc complexes (II).

The research includes the synthesis of new pyrazolines and oxazepine derivatives by reacting chalcones as raw materials with Isoniazid and 2-aminophenol, respectively, while chalcone compounds were prepared by the reaction of bromoacetophenone with a number of benzaldehyde substitutes. The structural formula of the synthesized compounds has been proven by measuring some physical properties such as melting point and spectroscopic methods such as infrared spectroscopy and nuclear magnetic resonance of proton and carbon. Biological activity of synthesized compounds (three concentrations) was evaluated using Staphylococcus aureus, Klebsiella pneumonia and pseudomonas, and comparison with isoniazid and gentamicin sulphate, the results encourage their use as important antibacterial.

The current study is conducted to estimate the level of the interleukin 22 concentration level and its relationship with some bacterial species in people who had wounds and surgeries. The study includes 40 samples of swabs and blood samples from patients with wound infections who attended Samarra General Hospital and some outpatient clinics, and their ages ranged between (12-68) years and of different sex, for the period from November 2021 to the end of March 2022. The information is recorded in a questionnaire for information about the person within the subject of the study. The samples are divided into wound infection samples for 30 surgical patients and control samples for the healthy 10 samples. The results of the current study show a significant decrease of P≤0.01 in the level of interleukin IL-22 concentration in patients who underwent surgical operations (13 pg/ml) compared to its level in control groups (37.13 pg/ml). The level of the concentration of the interleukin IL-22 decreases in the subjects with bacterial growth (Staph.aureus, Pseudomonas, Proteus, Klebsiella, E. coli) (14.66, 9.92, 17.08, 11.73, 11.67 pg/ml), respectively, and differently among people who had wounds and surgeries, as the results show that the level of IL-22 concentration decreases by different levels. Heterogeneous to those infected and according to the type of bacterial growth that appeared in them.

The use of preservatives in the field of food allows the provision of types of food products and foods in the off-season,ةIt also allows pharmaceutical and cosmetic products to be used for long periods without being damaged by the growth of microorganisms. But recently, several disadvantages of these compounds have emerged, including parabens, which include Propyl 4-hydroxybenzoate, due to their frequent use due to their availability in large quantities, cheap prices, and easy access. Several concentrations (800, 400, 200) mg/kg/day were used in this study for 30 days. as these concentrations affected the liver tissue of adult white male rats. The concentration of 800 mg/kg had the greatest effect on it, as it led to hepatocyte hypertrophy and degeneration, and cellular infiltration. Lymphocytic, hemosiderin, and Kupffer cell hyperplasia.

This study is conducted between 13/12/2021 to 5/5/2022 in the city of Samarra, and 83 blood samples are collected for people with leishmaniasis. Serological tests are carried out and it is found that 69.87% of those infected had specific antibodies IgM and 30.13% had IgG antibodies. The results of the study show the inhibitory efficacy of gold nanoparticles at size 0.15 on average growth of 1.56× 106 cells/ml in time 96, which inhibited the growth of the parasite since the start of the experiment at the probability level of p≤ 0.05 While the volume of 0.20 μL show a high inhibitory effect on the growth of the Promastigote of the leishmania parasite at an average growth of 0.85×106 cells / ml in time 72 from the start of the experiment at a significant level p≤ 0.05. The highest level of inhibitory effectiveness of the growth of the Promastigote of the f of the leishmania parasite is at the volume of 0.30 μL, where the average growth become 0.61 cells / ml. in the 48th time at the start of the experiment and this volume is the best size to affect the growth of the parasite in the agricultural medium compare to the effect of the drug Betamethasone, which inhibited the growth of the parasite at the concentration of 0.50 μL to 0.24×106 cells / ml at the 48th time from the start of the experiment at a significant level p≤ 0.05.

The current study is conducted between 13/12/2020 and 5/5/ 2021 Samarra General Hospital reviewed patients with symptoms of dermal leshmaniasis were collected. The results of this study show that there are moral differences in some of the studied variables. The results show that 30. 13% of infected people carry IgG and 69.87% carry IgM in the serum.Immunological tests have shown a moral rise at a morale level P < 0.05 in the rate of leukocyte IL- 10 in blood serum for dermatologic lysmania CL at 160.9 ± 44.4 pg/ml and 78.6 ± 20.3 pg/ml in uninfected people. The results show a moral rise of the TNF-α tumor necrosis factor at a moral level of p < 0.05 in the Lemania group compared to the healthy group, where the average injury was 154.5 ± 35.8 pg/mL in return. The control group recorded 99.2 ± 17.0 pg/Ml. The results showed a difference in the concentration of elements in the serum of people with leishmaniasis compared to the control group .the concentration of the selenium element 88.8 ± 13.5 ug/dl either its concentration in the control group 154.2 ± 16.2 ug/dl, The high copper concentration in infected people was ± 26.4 148.9 ug/dl while its There was no decrease in zinc level in the control group if the ratio is 98.9±19.1 ug/dl, The zinc element decreased its concentration in the serum of infected people to 90.8 ± 13.7 ug/dl compared to healthy 111.1.± 19.2 ug/dl.

The current study aimed to test the hepatic effect of strawberry fruits in male rabbits treated with paracetamol and to try to determine the mechanisms of this action on liver enzymes and some other factors under study. According to the findings, ceruloplasmin levels in blood serum significantly decreased as oxidative stress caused by paracetamol developed in the white male rabbit. The findings also showed a significant increase in phospholipids in the serum of acetaminophen-treated rabbits when compared to the healthy control group, as well as a significant rise in serum CK enzyme activity, alanine aminotransferase enzyme activity, and a significant rise in aspartate aminotransferase AST enzyme activity. And Significant variations in the activity of alkaline phosphatase in the blood serum of the rabbits treated with paracetamol compared to the healthy control group, together with a significant rise in the gamma-glutamyltransferase enzyme activity.

The aim of this paper is to construct the basic concept related to compactness in Double intuitionistic topological spaces (X,Ψ). We introduced the concepts of the Double intuitionistic compact and some of its types. Also, we found the relationships between these types with proofs and examples.

In this paper, we intend to study the concept of almost approximaitly nearlyprime submodules as new generalization of prime submodules, also generalization of approximaitly and nearly prime submodule. We give same basic properties, characterizations, and examples for this concept.

The experiment was conducted at the Lath house of the collage of Agriculture/ Tikrit University for the growing season 3/15/2019 to 2/15/2020 , to see the effect of spraying with kinetin growth regulator and addition of Humic acid on the characteristics of vegetative and root growth and the chemical content of two types of citrus fruits (shaddock and grapefruit), When shaddock and grapefruit seedlings were sprayed with three concentrations of the growth regulator kinetin (0, 75 and 150 mg. L-1.) And three levels of Humic acid were added (0, 5 and 10 ml.L-1), the addition and spraying were done on three dates of the appointment. The first date was 3/15/2019 and the second appointment 21 days after the first appointment, and so on for the third appointment. This study was carried out according to the Randomized Complete Block Design (R.C.B.D). The results were analyzed using a table of variance analysis, factors and their interactions were tested using the ready-made statistical program SAS and the lowest significant difference LSD was calculated at a probability level of 0.05. The results of the study are summarized as follows: The variety had a significant effect on the studied traits, as the grapefruit variety exceeded the rate of increase in leaves content of chlorophyll , nitrogen ,phosphor, potassium in leaves as it reached 12.22 mg.g-1 soft weight, 1.15%, 0.225% , 1.03% and 7.18% , while the shaddock variety gave the high rate for the carbohydrate / nitrogen as it reached 3.79 .The spraying with the growth regulator kinetin, especially the concentration of 150 mg / L-1, gave to a significant increase in the studied characteristics represented in the leaves content of chlorophyll , ,phosphor, potassium, carbohydrate and carbohydrate/ nitrogen in leaves , while the comparison treatment gave the lowest average for the aforementioned traits. Fertilization with humic acid, especially at the level of 10 ml. L-1, resulted in a significant increase in the rate of the leaves content of chlorophyll, nitrogen, phosphor, potassium, protein, carbohydrate and carbohydrate/ nitrogen in leaves, while the comparison treatment gave the lowest average for the aforementioned traits. The two and three interactions of the research factors showed significant differences for all the studied traits.

This study examined the current survey of the species of large families (Compositea, Chenopodiaceae, papilionaceae and crusifera) from Dicotyledons during the study period (2019-2020) in the area of Ain al-tamur disitrict, ther are (115) species which relate to (70) genus and (4) families. All these have been scientifically classified with their local and common or Arabic names. Besides their duration and economic importance (medical, toxis, nutritional, forage, artificial, harmful, aromatic, ornamental, fuelplant or other uses). Moreover, their geographical distribution the districts of Iraq and the study results statistics have shown that the vast majority of the collected species are horbal plants totalling (83) wild species out of (115) wild species. as for the shrub species it amounts to (18) wild species where as the number of woody species of tree is (3). As for the economic plants and their significance ,lets mention the fact that the number of the medical plants are (78)species,the plants used as forage amount to (87),the plants used as fuel are (16) species ,the toxic plants fall into (6),the ornamental plants are (20) species ,the aromatic plants are of (5) species , the weed plants (5)species , it also study the floristic composition ,there are clearly dominating to compositae families of (40) species.then the chenopodianaceae families with (30) species ,then the papilionaceae family with (24) species and the Crusifera family with (21) species so the dominating genus was Astragalus with (8) species ,then launaea with (7) species .

This study examined the current survey of the engiosperm plant of monocotyledon wild and cultivated during the study period (2019-2020) in the area of Ain al-tamur disitrict, ther are (66) species which relate to (9) families. All these have been scientifically classified with their local and common or Arabic names. Besides their duration and economic importance (medical, toxis, nutritional, forage, artificial, harmful, aromatic, ornamental, fuelplant or other uses). Moreover, their geographical distribution the districts of Iraq and the study results statistics have shown that the vast majority of the collected species are horbal plants totalling (40) wild species out of (66) wild species. as for the shrub species it amounts to (1) wild species where as the number of woody species of tree is (2), the perennial plant (23) the biennial plant (3) species. As for the economic plants and their significance, lets mention the fact that the number of the medical plants are (17) species,the plants used as forage amount to (52),the plants used as fuel are (2) species , the ornamental plants are (4) species , it also study the floristic composition ,there are clearly dominating to Graminae family of (44) species .then the Cyperaceae families with (5)species ,then the Juncaceae family with (3) species. so the dominating genus was Bromus with (4) species, then Juncus and Aleuropus. the plant communities was studied, there are dominating to wild species as Eragrostis cilianensis , Phragmites aystralis and the dominating cultivated species phoenix sp. In (4), (7), (12), (13) point and the triticum sp. In (4), (7), (12), (13) point.

The study aimed to prepare physical _ preventive exercises to strengthen the posterior muscle of the thigh (popliteus) in order to develop some aspects of strength and to contribute to the prevention of injuries during training or competition. In the study, three tests were used for the two men, the first was three hopscotches with the right leg and the left leg, the second was the posterior Maxillary half test with iron to measure the maximum strength, and the third was a 30-meter running test from the flying position to measure the transitional speed. The researchers concluded that the special exercises contributed to the development of the range of motion and elongation of the posterior thigh muscle (popliteus) and thus also contributed to the development of transitional speed at a good rate, as well as the maximum strength, strength and explosiveness of the muscles of the two legs.